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In the synthesis of MOF-5 at room temperature, 4.39 g of Zn(NO3)2·6H2O (14.76 mmol) was dissolved in 55.5 g of DMF, and 0.43 g of Na2BDC (2.05 mmol), was dissolved in other 55.5 g of DMF. The metal salt solution was added to the linker solution under continuous stirring and the resulting solution was stirred for 24 h.
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