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Metry Open-File Report 02 462 U.S. Department of the Interior U.S. Geological Survey Methods of Analysis by the U.S. Geological Survey National Water Quality Laboratory A Method Supplement for the Determination of Fipronil and Degradates in Water by Gas Chromatography/Mass Spectrometry By James E. Madsen, Mark W. Sandstrom, and Steven D. Zaugg U.S.

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